5AFL
alpha7-AChBP in complex with lobeline and fragment 3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Collection date | 2013-04-02 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.808, 112.300, 143.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.829 - 2.385 |
R-factor | 0.1738 |
Rwork | 0.171 |
R-free | 0.23100 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.123 |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.910 |
High resolution limit [Å] | 2.350 |
Rmerge | 0.080 |
Number of reflections | 58398 |
<I/σ(I)> | 15.8 |
Completeness [%] | 99.8 |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |