5A9P
Crystal structure of Operophtera brumata CPV18 polyhedra
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 3 |
Unit cell lengths | 102.770, 102.770, 102.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 72.669 - 1.476 |
R-factor | 0.1311 |
Rwork | 0.130 |
R-free | 0.14750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oh6 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.146 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.700 | 1.510 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.320 | |
Number of reflections | 30415 | |
<I/σ(I)> | 7.1 | 1.5 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 12.9 | 8.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | PH 7.5 |