5A7Z
Crystal structure of Sulfolobus acidocaldarius Trm10 at 2.1 angstrom resolution.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-11 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.770, 46.320, 138.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.110 - 2.100 |
R-factor | 0.22594 |
Rwork | 0.224 |
R-free | 0.26413 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a7t |
RMSD bond length | 0.014 |
RMSD bond angle | 1.308 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.900 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.010 | 0.120 |
Number of reflections | 16213 | |
<I/σ(I)> | 9.23 | 1.74 |
Completeness [%] | 99.4 | 99 |
Redundancy | 8.6 | 4.68 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 2 % DIOXANE, 0.05 M BICINE PH 9, 15 % PEG20K |