5A3E
2.5A structure of lysozyme determined by MicroED with data from a single crystal
Experimental procedure
Temperature [K] | 100 |
Collection date | 2014-02-05 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 75.890, 75.890, 36.930 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 11.189 - 2.501 |
R-factor | 0.2152 |
Rwork | 0.213 |
R-free | 0.25310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3j6k |
RMSD bond length | 0.003 |
RMSD bond angle | 0.687 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 11.200 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.292 | |
Number of reflections | 3116 | |
Completeness [%] | 80.1 | 80.1 |
Redundancy | 3.4 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | pH 4.5 |