4ZZB
The GLIC pentameric Ligand-Gated Ion Channel Locally-closed form complexed to xenon
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-07-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.2 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 176.966, 130.528, 157.526 |
Unit cell angles | 90.00, 100.33, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.400 |
R-factor | 0.2166 |
Rwork | 0.216 |
R-free | 0.22260 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.990 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | BUSTER (2.11.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.620 | 3.580 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.052 | 0.586 |
Number of reflections | 47834 | |
<I/σ(I)> | 12 | 1.8 |
Completeness [%] | 98.4 | 97.1 |
Redundancy | 3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 290 | 12-15 % PEG4000 0.1M Na Acetate pH4 0.4M NaSCN 15% glycerol 5% DMSO |