4ZUZ
SidC 1-871
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-06-30 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9759 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 228.159, 83.934, 129.405 |
| Unit cell angles | 90.00, 108.82, 90.00 |
Refinement procedure
| Resolution | 49.160 - 2.860 |
| R-factor | 0.2274 |
| Rwork | 0.225 |
| R-free | 0.28150 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4irh |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.475 |
| Data scaling software | HKL-2000 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.860 |
| Number of reflections | 53345 |
| <I/σ(I)> | 46.5 |
| Completeness [%] | 100.0 |
| Redundancy | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | PEG 8000, Hepes, NaCl |
