4ZQY
Ringhalexin from hemachatus haemachatus: A novel inhibitor of extrinsic tenase complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2012-05-11 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54178 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 82.160, 82.160, 82.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.951 |
R-factor | 0.2197 |
Rwork | 0.217 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2h8u |
RMSD bond length | 0.009 |
RMSD bond angle | 1.599 |
Data reduction software | MOSFLM |
Data scaling software | MOSFLM |
Phasing software | BALBES |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 |
High resolution limit [Å] | 2.951 |
Number of reflections | 6253 |
<I/σ(I)> | 14.7 |
Completeness [%] | 99.4 |
Redundancy | 8.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 29% MPD, 0.1M HEPES |