4ZN3
Crystal Structure of MjSpt4:Spt5 complex conformation B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.395, 88.943, 91.955 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.300 |
R-factor | 0.22885 |
Rwork | 0.227 |
R-free | 0.25569 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zn1 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.172 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.480 | |
Number of reflections | 17139 | |
<I/σ(I)> | 15.5 | 3.3 |
Completeness [%] | 99.4 | 100 |
Redundancy | 4.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | PEG 6000, MPD, MES |