4ZK3
Psoriasis pathogenesis - Pso p27 constitute a compact structure forming large aggregates. Low pH structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-05-07 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.87260 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 53.161, 68.843, 104.260 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.450 - 2.000 |
| R-factor | 0.18415 |
| Rwork | 0.181 |
| R-free | 0.24370 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.819 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.450 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.078 | 0.601 |
| Number of reflections | 26612 | |
| <I/σ(I)> | 14.9 | 2.6 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 6.6 | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 298 | 27% PEGMME 2K, 0.1 M Na acetate pH 4.5 |
