4ZHD
Siderocalin-mediated recognition and cellular uptake of actinides
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 114.589, 114.589, 118.781 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.050 |
R-factor | 0.2047 |
Rwork | 0.204 |
R-free | 0.22570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lm6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.146 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | REFMAC (5.8.0049) |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.090 |
High resolution limit [Å] | 2.050 | 5.560 | 2.050 |
Rmerge | 0.063 | 0.037 | 0.368 |
Total number of observations | 472916 | ||
Number of reflections | 49864 | ||
<I/σ(I)> | 22.1 | ||
Completeness [%] | 99.1 | 95.8 | 95.3 |
Redundancy | 9.5 | 8.9 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4 | 298 | NaCl, Li2SO4, Acetate, Ammonium Sulfate |