4ZC3
DNA binding domain of small terminase SF6 phage
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | H 3 |
Unit cell lengths | 52.545, 52.545, 54.877 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.270 - 1.400 |
R-factor | 0.1994 |
Rwork | 0.199 |
R-free | 0.21310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.589 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.300 | 1.440 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.019 | 1.052 |
Number of reflections | 11127 | |
<I/σ(I)> | 33.67 | 1.42 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 5.1 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291.15 | PACT premier screen (Molecular Dimensions) B2 0.1 M Malonate-Imidazole-Borate buffer 25 % w/v PEG 1500 |