4ZBT
Streptomyces bingchenggensis aldolase-dehydratase in Schiff base complex with pyruvate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-05 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 156.911, 123.487, 52.932 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.900 - 1.800 |
R-factor | 0.1678 |
Rwork | 0.166 |
R-free | 0.20810 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.317 |
Data reduction software | HKL-2000 (2.3.10) |
Data scaling software | HKL-2000 (2.3.10) |
Refinement software | PHENIX (dev_1965) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.900 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.102 | 0.334 |
Number of reflections | 92220 | |
<I/σ(I)> | 12.3 | 1.7 |
Completeness [%] | 95.4 | 64 |
Redundancy | 3.1 | 1.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.1 | 295 | 3.4-3.7 M Potassium formate, 0.1 M bis-tris propane, pH 9.1 |