4ZB0
A dehydrated form of glucose isomerase collected at room temperature.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2015-02-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 83.485, 95.020, 98.484 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 68.380 - 2.000 |
R-factor | 0.1393 |
Rwork | 0.137 |
R-free | 0.17969 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mnz |
RMSD bond length | 0.022 |
RMSD bond angle | 2.371 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.380 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.060 | 0.138 |
Total number of observations | 169888 | |
Number of reflections | 53324 | |
<I/σ(I)> | 10.4 | 5.9 |
Completeness [%] | 99.5 | 99.6 |
Redundancy | 3.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.1 M Hepes, 10% PEG 400, 0.05 M Manganese Chloride, 20% Glucose |