4Z8Q
CRYSTAL STRUCTURE OF AvrRxo1-ORF1:AvrRxo1-ORF2 COMPLEX, SELENOMETHIONINE SUBSTITUTED.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 75.589, 88.869, 153.488 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.060 - 1.890 |
R-factor | 0.229 |
Rwork | 0.226 |
R-free | 0.27300 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.401 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.950 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.086 | |
Number of reflections | 39222 | |
<I/σ(I)> | 26.2 | 7.3 |
Completeness [%] | 86.0 | |
Redundancy | 13.9 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.8 M NAH2PO4, 0.8 M KH2PO4, 15% GLYCEROL, 8 MM DTT, 0.1 M HEPES, , PH 7.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K |