4Z1H
Crystal structure of human Trap1 with SMTIN-P01
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-11-14 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 69.336, 69.336, 255.774 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 34.354 - 2.900 |
| R-factor | 0.2382 |
| Rwork | 0.235 |
| R-free | 0.28530 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.987 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 35.000 |
| High resolution limit [Å] | 2.900 |
| Number of reflections | 14775 |
| <I/σ(I)> | 23.4 |
| Completeness [%] | 99.8 |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 16% PEG 8K, 100mM calcium acetate, 100mM sodium cacodylate. |
