4YYA
The structure of hemagglutinin from a H6N1 influenza virus (A/Taiwan/2/2013) in complex with avian receptor analog 3'SLNLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-09-10 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.07138 |
| Spacegroup name | P 63 |
| Unit cell lengths | 114.194, 114.194, 164.962 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 46.946 - 2.595 |
| R-factor | 0.1834 |
| Rwork | 0.182 |
| R-free | 0.20820 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.037 |
| Data reduction software | SCALA |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.690 |
| High resolution limit [Å] | 2.595 | 2.600 |
| Rmerge | 0.126 | 0.494 |
| Number of reflections | 37568 | |
| <I/σ(I)> | 22 | 6.8 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 13.1 | 13.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.2M ammonium acetate, 0.1M sodium acetate pH4.0, 15%(w/v) PEG4000 |
