4YUA
Glycogen phosphorylase in complex with ellagic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2014-12-04 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.04 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.480, 128.480, 116.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.350 - 2.000 |
R-factor | 0.17428 |
Rwork | 0.173 |
R-free | 0.20178 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.009 |
RMSD bond angle | 1.297 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.350 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 63707 | |
<I/σ(I)> | 5.6 | 2.7 |
Completeness [%] | 97.2 | 98.8 |
Redundancy | 3.4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.8 | 289 | 10mM BES buffer |