4YSC
Completely oxidized structure of copper nitrite reductase from Alcaligenes faecalis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SACLA BEAMLINE BL3 |
Synchrotron site | SACLA |
Beamline | BL3 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2014-11-24 |
Detector | MPCCD |
Wavelength(s) | 1.771 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.100, 103.800, 147.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.900 - 2.030 |
R-factor | 0.16583 |
Rwork | 0.164 |
R-free | 0.20302 |
RMSD bond length | 0.020 |
RMSD bond angle | 1.898 |
Data reduction software | CrystFEL |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 73.900 |
High resolution limit [Å] | 2.030 |
Number of reflections | 61011 |
<I/σ(I)> | 6.97 |
Completeness [%] | 100.0 |
Redundancy | 147 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | 100 mM sodium acetate pH 4.0, 10% PEG 4000 |