4YO3
Enteroaggregative Escherichia Coli TssA N-terminal fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-28 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.987 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 134.130, 178.050, 106.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.390 - 3.370 |
R-factor | 0.2507 |
Rwork | 0.250 |
R-free | 0.26140 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.180 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHELXDE |
Refinement software | BUSTER (2.10.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.400 | 3.470 |
High resolution limit [Å] | 3.370 | 3.370 |
Rmerge | 0.150 | 0.720 |
Number of reflections | 36779 | |
<I/σ(I)> | 11.4 | 2.4 |
Completeness [%] | 99.7 | 99.9 |
Redundancy | 7.8 | 7.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 300 nL of protein at 4.7 mg/mL with 100 nL of 29% PEG 3350, 0.1 M Hepes pH 7.5 |