4YNN
Structure of Legionella pneumophila DegQ (S190A variant)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.979 |
Spacegroup name | P 63 |
Unit cell lengths | 147.909, 147.909, 383.514 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.543 - 3.200 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.21930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pv2 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.862 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.543 | 3.280 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.100 | 0.547 |
Number of reflections | 77028 | |
<I/σ(I)> | 14.5 | 2.1 |
Completeness [%] | 99.0 | 94.5 |
Redundancy | 7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 100 mM citrate pH5.5; 17.5% (w/v) PEG 400 |