4YL4
1.1 Angstrom resolution X-ray Crystallographic Structure of Psudoazurin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-24 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 56.019, 63.200, 67.045 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.040 - 1.100 |
R-factor | 0.14951 |
Rwork | 0.148 |
R-free | 0.18571 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bqk |
RMSD bond length | 0.025 |
RMSD bond angle | 2.418 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.140 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.060 | |
Number of reflections | 47290 | |
<I/σ(I)> | 0.34 | 4 |
Completeness [%] | 97.1 | 99.6 |
Redundancy | 7 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 30% PEG 4000, 0.1 M Tris, 0.1M magnesium chloride, 5% Glycerol |