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4YKK

Mnemiopsis leidyi ML032222a iGluR LBD D-serine complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]100
Detector technologyCCD
Collection date2013-12-02
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1.000
Spacegroup nameP 1 21 1
Unit cell lengths45.951, 123.753, 54.505
Unit cell angles90.00, 111.78, 90.00
Refinement procedure
Resolution35.128 - 1.380
R-factor0.1449
Rwork0.144
R-free0.16720
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)4yki
RMSD bond length0.009
RMSD bond angle1.233
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.9_1692))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0001.400
High resolution limit [Å]1.3801.380
Rmerge0.0650.610
Number of reflections115480
<I/σ(I)>19.51.7
Completeness [%]99.695.6
Redundancy3.72.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5277Reservoir: 25% PEG 8K, 100 mM Cacodylate, 150 mM MgS04. Protein buffer: 100 mM NaCl, 10 mM HEPES, pH 7.0, 0.5 mM EDTA, 100 mM D-Serine, no added glycine

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