4YHV
Yeast Prp3 C-terminal fragment 325-469
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-30 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.91841 |
Spacegroup name | P 65 |
Unit cell lengths | 56.079, 56.079, 86.753 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.283 - 2.000 |
R-factor | 0.164 |
Rwork | 0.161 |
R-free | 0.22080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4yhu |
RMSD bond length | 0.013 |
RMSD bond angle | 1.278 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.120 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.068 | 0.439 |
Number of reflections | 10459 | |
<I/σ(I)> | 24.96 | 5.94 |
Completeness [%] | 99.3 | 96.2 |
Redundancy | 11.4 | 11.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M HEPES, pH 7.5, 10 % PEG 8000 |