4YGM
Vaccinia virus his-D4/A20(1-50) in complex with uracil
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9786 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 92.786, 92.786, 146.744 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 80.360 - 1.850 |
R-factor | 0.19229 |
Rwork | 0.191 |
R-free | 0.22248 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4od8 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.628 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.000 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.052 | 0.597 |
Number of reflections | 63182 | |
<I/σ(I)> | 23.2 | 3.6 |
Completeness [%] | 96.4 | 94 |
Redundancy | 7.5 | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.7 | 293 | 0.1M bicine, 1.5M ammonium sulfate |