4YFT
HUab-20bp
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 12.3.1 |
Synchrotron site | ALS |
Beamline | 12.3.1 |
Temperature [K] | 93.15 |
Detector technology | CCD |
Collection date | 2013-01-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 83.036, 83.036, 63.114 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.720 - 2.914 |
R-factor | 0.2162 |
Rwork | 0.215 |
R-free | 0.25110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mul |
RMSD bond length | 0.010 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | BUSTER-TNT (BUSTER 2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.036 | 2.924 |
High resolution limit [Å] | 2.914 | 2.914 |
Rmerge | 0.153 | 2.187 |
Total number of observations | 141920 | |
Number of reflections | 5183 | |
<I/σ(I)> | 23.2 | 2.188 |
Completeness [%] | 99.9 | 100 |
Redundancy | 27.4 | 29.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 298 | 0.1M Bis-Tris pH 6.5, 30% PEG MME 550, 0.05 M CaCl2 |