4YB7
Adenosine triphosphate phosphoribosyltransferase from Campylobacter jejuni in complex with ATP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2014-04-02 |
| Detector | ADSC QUANTUM 210r |
| Wavelength(s) | 0.959 |
| Spacegroup name | P 1 |
| Unit cell lengths | 91.667, 91.835, 154.903 |
| Unit cell angles | 101.11, 95.21, 118.14 |
Refinement procedure
| Resolution | 50.000 - 2.200 |
| R-factor | 0.23248 |
| Rwork | 0.231 |
| R-free | 0.25429 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.471 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.240 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.076 | 0.800 |
| Number of reflections | 212958 | |
| <I/σ(I)> | 2 | 1.6 |
| Completeness [%] | 98.1 | 97.3 |
| Redundancy | 3.9 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293.15 | Sodium Acetate, Magnesium Chloride, PEG4000, ATP |
