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4YB0

3',3'-cGAMP riboswitch bound with c-di-GMP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]100
Detector technologyCCD
Collection date2014-08-14
DetectorADSC QUANTUM 315r
Wavelength(s)0.9792
Spacegroup nameC 1 2 1
Unit cell lengths174.829, 44.901, 68.210
Unit cell angles90.00, 103.33, 90.00
Refinement procedure
Resolution85.100 - 2.121
R-factor0.2297
Rwork0.228
R-free0.26200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4yaz
RMSD bond length0.007
RMSD bond angle1.457
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.9_1692))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]85.1002.240
High resolution limit [Å]2.1202.120
Rmerge0.044
Number of reflections28937
<I/σ(I)>16.31.3
Completeness [%]98.197.9
Redundancy3.33.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.52930.1 M Na/K-phosphate, pH 6.2-6.6, 0.2 M NaCl and 40-45% PEG400

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