4YAV
Crystal structure of LigG in complex with B-glutathionyl-acetoveratrone (GS-AV) from Sphingobium sp. strain SYK-6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97741 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 64.543, 64.543, 120.880 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.037 - 1.401 |
R-factor | 0.1402 |
Rwork | 0.139 |
R-free | 0.16420 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.558 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.037 |
High resolution limit [Å] | 1.400 |
Number of reflections | 58125 |
<I/σ(I)> | 23.8 |
Completeness [%] | 100.0 |
Redundancy | 10.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 0.1 M Bis-Tris propane pH 7.0, 1.5 M Ammonium Sulfate |