4YAM
Crystal structure of LigE-apo form from Sphingobium sp. strain SYK-6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-02-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.99996 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 122.556, 97.155, 131.387 |
Unit cell angles | 90.00, 106.65, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.905 |
R-factor | 0.228 |
Rwork | 0.227 |
R-free | 0.27130 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.956 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8.3_1479)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 114153 |
<I/σ(I)> | 9 |
Completeness [%] | 99.2 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M Ammonium Citrate, 0.1 M MES pH 5.5, 20 % PEG 3,350, 5% Isopropanol |