4Y9R
rat CYPOR mutant - G141del
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-04-06 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 102.026, 115.886, 119.655 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.710 - 2.400 |
R-factor | 0.195 |
Rwork | 0.195 |
R-free | 0.25400 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.710 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.074 |
Number of reflections | 56024 |
<I/σ(I)> | 32 |
Completeness [%] | 99.9 |
Redundancy | 9.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 292 | PEG 4000, Sodium Acetate, HEPES |