4Y9R

rat CYPOR mutant - G141del

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2012-04-06
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	102.026, 115.886, 119.655
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.710 - 2.400
R-factor	0.195
Rwork	0.195
R-free	0.25400
RMSD bond length	0.006
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	CNS (1.3)

Data quality characteristics

	Overall
Low resolution limit [Å]	37.710
High resolution limit [Å]	2.400
Rmerge	0.074
Number of reflections	56024
<I/σ(I)>	32
Completeness [%]	99.9
Redundancy	9.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	292	PEG 4000, Sodium Acetate, HEPES