4Y7U

Structural analysis of MurU

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	93.2
Detector technology	PIXEL
Collection date	2014-02-07
Detector	DECTRIS PILATUS 2M
Wavelength(s)	1.0
Spacegroup name	P 61 2 2
Unit cell lengths	72.750, 72.750, 163.130
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.861 - 1.700
R-factor	0.2296
Rwork	0.228
R-free	0.26400
RMSD bond length	0.008
RMSD bond angle	1.192
Data reduction software	XDS
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.700
Number of reflections	28941
<I/σ(I)>	30.72
Completeness [%]	100.0
Redundancy	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	293	(NH4)2SO4, MES