4Y7U
Structural analysis of MurU
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93.2 |
Detector technology | PIXEL |
Collection date | 2014-02-07 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 72.750, 72.750, 163.130 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.861 - 1.700 |
R-factor | 0.2296 |
Rwork | 0.228 |
R-free | 0.26400 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.192 |
Data reduction software | XDS |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.700 |
Number of reflections | 28941 |
<I/σ(I)> | 30.72 |
Completeness [%] | 100.0 |
Redundancy | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | (NH4)2SO4, MES |