4Y7T

Structural analysis of MurU

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	93.2
Detector technology	PIXEL
Collection date	2012-07-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.0
Spacegroup name	P 61 2 2
Unit cell lengths	72.610, 72.610, 158.470
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.446 - 1.800
R-factor	0.2132
Rwork	0.211
R-free	0.24550
RMSD bond length	0.015
RMSD bond angle	1.526
Data reduction software	XDS
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.800
Number of reflections	23700
<I/σ(I)>	13.31
Completeness [%]	99.9
Redundancy	9.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	293	(NH4)2SO4, MES