4Y7I

Crystal Structure of MTMR8

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2012-06-15
Detector	ADSC QUANTUM 210r
Wavelength(s)	1.00
Spacegroup name	P 21 21 21
Unit cell lengths	69.573, 77.188, 197.793
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.637 - 2.802
R-factor	0.1803
Rwork	0.177
R-free	0.24670
RMSD bond length	0.009
RMSD bond angle	1.163
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	REFMAC
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.850
High resolution limit [Å]	2.800	2.800
Rmerge		0.489
Number of reflections	26992
<I/σ(I)>	17	2.65
Completeness [%]	100.0	100
Redundancy	5.8	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	10mM N-(2-Acetamido)iminodiacetic acid, 1.0M ammonium phosphate dibasic