4Y2I
Gold ion bound to GolB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-03-04 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 37.093, 37.093, 169.911 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.560 - 2.000 |
R-factor | 0.22867 |
Rwork | 0.227 |
R-free | 0.26638 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.853 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.455 | |
Number of reflections | 7169 | |
<I/σ(I)> | 51 | 2.2 |
Completeness [%] | 99.0 | 86.2 |
Redundancy | 10.6 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 2.0 M Ammonium citrate tribasic, 0.1 M BIS-TRIS propane |