4Y0N
SAV1875
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-27 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.23986 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 81.455, 95.004, 42.648 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.780 - 2.100 |
R-factor | 0.19291 |
Rwork | 0.191 |
R-free | 0.22649 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oi4 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.052 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 2.100 |
Number of reflections | 19995 |
<I/σ(I)> | 39.2 |
Completeness [%] | 99.5 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 29% PEG mme2000, 100mM Bis-Tris |