4XZS
Crystal Structure of TRIAP1-MBP fusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-22 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.390, 56.010, 100.280 |
Unit cell angles | 90.00, 106.35, 90.00 |
Refinement procedure
Resolution | 48.410 - 2.120 |
R-factor | 0.19813 |
Rwork | 0.196 |
R-free | 0.24163 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hsj |
RMSD bond length | 0.013 |
RMSD bond angle | 1.470 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.410 | 2.180 |
High resolution limit [Å] | 2.120 | 2.120 |
Rmerge | 0.093 | 0.585 |
Number of reflections | 45307 | |
<I/σ(I)> | 9.3 | 2.2 |
Completeness [%] | 98.7 | 94 |
Redundancy | 3.6 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 100 mM sodium acetate, 25% (w/v) PEG 4000, 18% (w/v) MPD, 200 mM ammonium sulphate |