4XVW
Crystal structure of Proteus mirabilis ScsC in a compact conformation
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-06-23 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9792 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 137.475, 163.885, 181.936 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 91.152 - 2.600 |
| R-factor | 0.254 |
| Rwork | 0.248 |
| R-free | 0.28180 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.212 |
| Data reduction software | XDS (January 10, 2014) |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 91.200 | 2.740 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.072 | 0.617 |
| Number of reflections | 243466 | |
| <I/σ(I)> | 11 | 2 |
| Completeness [%] | 98.6 | 95.4 |
| Redundancy | 3.8 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.8 | 293 | 2.85 M sodium malonate, 0.1 M Cobalt(II)chloride hexahydrate |
