4XV8
CcP gateless cavity
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 273 |
Detector technology | CCD |
Collection date | 2011-09-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95372 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.460, 76.950, 107.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.760 - 1.570 |
R-factor | 0.11 |
Rwork | 0.108 |
R-free | 0.14000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.592 |
Data reduction software | xia2 (0.3.3.3) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.760 | 1.610 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.053 | 0.555 |
Number of reflections | 60219 | |
<I/σ(I)> | 14.9 | 2.4 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 4.3 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 283 | Compound soaked into crystal grown in equal volume of 500mM MES buffer and 25% MPD |