4XV6

CcP gateless cavity

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	273
Detector technology	CCD
Collection date	2011-12-11
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.95372
Spacegroup name	P 21 21 21
Unit cell lengths	51.480, 76.520, 107.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.420 - 1.550
R-factor	0.105
Rwork	0.104
R-free	0.13600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.019
RMSD bond angle	1.646
Data reduction software	xia2 (0.3.3.3)
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.420	1.590
High resolution limit [Å]	1.550	1.550
Rmerge	0.040	0.649
Number of reflections	62017
<I/σ(I)>	17	2.2
Completeness [%]	99.7	99.7
Redundancy	4	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	283	CRYSTAL GROWN IN EQUAL VOLUME OF 500mM MES BUFFER AND 25% MPD