4XU6
Crystal structure of cross-linked MvINS R77C trimer at 1.9A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | H 3 |
Unit cell lengths | 85.596, 85.596, 126.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.071 - 1.898 |
R-factor | 0.1895 |
Rwork | 0.189 |
R-free | 0.20320 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.117 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 1.898 |
Number of reflections | 26955 |
<I/σ(I)> | 29.8 |
Completeness [%] | 98.9 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG 400 |