Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-08-26 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.979740 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 131.443, 205.298, 234.410 |
| Unit cell angles | 90.00, 94.10, 90.00 |
Refinement procedure
| Resolution | 48.828 - 3.796 |
| R-factor | 0.2862 |
| Rwork | 0.285 |
| R-free | 0.29940 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.241 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.830 | 3.860 |
| High resolution limit [Å] | 3.790 | 3.790 |
| Rmerge | 0.383 | 3.826 |
| Number of reflections | 243648 | |
| <I/σ(I)> | 8.8 | 0.9 |
| Completeness [%] | 99.3 | 87.5 |
| Redundancy | 20 | 16.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M CHES, pH 9.2, 29% v/v PEG400 |
