4XPM
Crystal structure of EGO-TC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-28 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9794 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 48.118, 48.118, 223.377 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.414 - 2.400 |
R-factor | 0.1728 |
Rwork | 0.171 |
R-free | 0.21670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ftx 3ms6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.087 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.076 | 0.520 |
Number of reflections | 11033 | |
<I/σ(I)> | 18.7 | 4.6 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 6.2 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 0.2M NaCl, 0.1M Bis-Tris (pH 5.5), 25% PEG 3350 |