4XOW
Structure of rsGreen0.7 in the green-on-state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-11 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.758, 61.594, 105.703 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.110 - 1.250 |
R-factor | 0.1416 |
Rwork | 0.141 |
R-free | 0.16490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.339 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.110 | 1.290 |
High resolution limit [Å] | 1.250 | 1.250 |
Rmerge | 0.077 | 0.670 |
Number of reflections | 109670 | |
<I/σ(I)> | 9.7 | 1.9 |
Completeness [%] | 98.8 | 99.6 |
Redundancy | 3.3 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 289 | 0.1 M Tris pH 8.5, 25% PEG 3350 |