4XN6
Crystal structure at room temperature of hen-egg lysozyme in complex with benzamidine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2014-07-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9797 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.292, 79.292, 38.073 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.100 - 1.350 |
| R-factor | 0.1397 |
| Rwork | 0.138 |
| R-free | 0.16550 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.239 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.100 |
| High resolution limit [Å] | 1.350 |
| Number of reflections | 21988 |
| <I/σ(I)> | 2.5 |
| Completeness [%] | 99.5 |
| Redundancy | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | NaOAc 100mM ,4% (w/v) NaCl |
