4XM5
C. glabrata Slx1.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-05-30 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.280 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 57.486, 57.486, 183.642 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.725 - 2.340 |
| R-factor | 0.1972 |
| Rwork | 0.191 |
| R-free | 0.25060 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.105 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.480 |
| High resolution limit [Å] | 2.340 | 2.340 |
| Rmerge | 0.098 | 0.671 |
| Number of reflections | 24808 | |
| <I/σ(I)> | 13.31 | 2.38 |
| Completeness [%] | 100.0 | 99.7 |
| Redundancy | 6.9 | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1.4 M sodium citrate tribasic dihydrate and 0.1 M HEPES-NaOH (pH 7.5) |
