4XK8
Crystal structure of plant photosystem I-LHCI super-complex at 2.8 angstrom resolution
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-12-11 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 165.624, 192.220, 175.089 |
| Unit cell angles | 90.00, 91.41, 90.00 |
Refinement procedure
| Resolution | 49.147 - 2.800 |
| R-factor | 0.2123 |
| Rwork | 0.210 |
| R-free | 0.24760 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.401 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.800 |
| Number of reflections | 268282 |
| <I/σ(I)> | 7 |
| Completeness [%] | 99.8 |
| Redundancy | 7.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 285 | PEG |
