4XJ1
Crystal structure of Vibrio cholerae DncV apo form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-15 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 0.97906 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.998, 50.742, 73.072 |
| Unit cell angles | 90.00, 93.07, 90.00 |
Refinement procedure
| Resolution | 47.329 - 1.770 |
| R-factor | 0.1814 |
| Rwork | 0.180 |
| R-free | 0.20390 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.137 |
| Data reduction software | HKL-2000 |
| Phasing software | SHARP |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.770 |
| Number of reflections | 42361 |
| <I/σ(I)> | 60 |
| Completeness [%] | 99.3 |
| Redundancy | 15.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | PEG3350, sodium fluoride, Bis-Tris propane |
