4XID
AntpHD with 15bp DNA duplex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 85 |
Detector technology | IMAGE PLATE |
Collection date | 2014-04-25 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 96.443, 96.443, 90.142 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.601 - 2.701 |
R-factor | 0.2285 |
Rwork | 0.224 |
R-free | 0.27430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 9ant |
RMSD bond length | 0.005 |
RMSD bond angle | 0.746 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX ((phenix.refine: dev_1810)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.750 |
High resolution limit [Å] | 2.700 | 7.320 | 2.700 |
Rmerge | 0.054 | 0.018 | |
Total number of observations | 94639 | ||
Number of reflections | 12086 | ||
<I/σ(I)> | 12.7 | ||
Completeness [%] | 99.0 | 98.9 | 97.3 |
Redundancy | 7.8 | 6.8 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 300 | 20 mM BTP, 10 mM NiCl, 5% MPD |