4XI6
Crystal structure of the MZM-REP domains of Mind bomb 1
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.2562, 1.2822, 1.283 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 73.083, 73.083, 170.959 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.939 - 2.040 |
R-factor | 0.2111 |
Rwork | 0.208 |
R-free | 0.24810 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.967 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.080 |
High resolution limit [Å] | 2.040 | 5.540 | 2.040 |
Rmerge | 0.067 | 0.038 | 0.404 |
Total number of observations | 235966 | ||
Number of reflections | 29269 | ||
<I/σ(I)> | 6.5 | ||
Completeness [%] | 95.2 | 95.2 | 53.6 |
Redundancy | 8.1 | 8.2 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293.15 | 1.5 M (NH4)2SO4, 20% v/v glycerol, HEPES pH 7.6 |