4XHW
Crystal structure of Timeless_PAB domain in SeMet-labelled form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97923 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 66.597, 100.083, 149.581 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.930 - 2.850 |
R-factor | 0.1954 |
Rwork | 0.193 |
R-free | 0.25340 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.397 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 24.930 |
High resolution limit [Å] | 2.850 |
Number of reflections | 12777 |
<I/σ(I)> | 27.1 |
Completeness [%] | 100.0 |
Redundancy | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 298 | 25% PEG 3350, 200mM sodium acetate |